Methoxyacetyl chloride
Methoxyacetyl chloride
CAS: 38870-89-2
Molecular Formula: C3H5ClO2
Methoxyacetyl chloride - Names and Identifiers
| Name | Methoxyacetyl chloride |
| Synonyms | NSC 82321 Methoxyacetyl chloride MEYHOXY ACETYL CHLORIDE 2-methoxyacetyl chloride Acetyl chloride, methoxy- 2'-deoxy-5-hydroxyuridine METHOXYACETYL CHLORIDE, STAB. Methoxyacetyl chloride, stabilized Methoxyacetyl Chloride [Chloromethylating Reagent] |
| CAS | 38870-89-2 |
| EINECS | 254-169-2 |
| InChI | InChI=1/C3H5ClO2/c1-6-2-3(4)5/h2H2,1H3 |
| InChIKey | JJKWHOSQTYYFAE-UHFFFAOYSA-N |
Methoxyacetyl chloride - Physico-chemical Properties
| Molecular Formula | C3H5ClO2 |
| Molar Mass | 108.52 |
| Density | 1.187 g/mL at 25 °C (lit.) |
| Boling Point | 112-113 °C (lit.) |
| Flash Point | 84°F |
| Water Solubility | reacts |
| Solubility | Miscible with acetone, ether, carbon tetrachloride and chloroform. |
| Vapor Presure | 21.7mmHg at 25°C |
| Appearance | Liquid |
| Color | Clear colorless to yellow |
| BRN | 1740244 |
| Storage Condition | 2-8°C |
| Sensitive | Moisture Sensitive |
| Refractive Index | n20/D 1.419(lit.) |
| Physical and Chemical Properties | Methoxyacetyl chloride is colorless liquid, flammable and corrosive, B. p.112 ~ 113 ℃,n20D 1.4190, relative density of 1.187, soluble in ether, benzene, ketone and other organic solvents. |
| Use | Used as pharmaceutical and dye intermediates |
Methoxyacetyl chloride - Risk and Safety
| Hazard Symbols | C - Corrosive |
| Risk Codes | R10 - Flammable R34 - Causes burns R36/37 - Irritating to eyes and respiratory system. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 - Wear suitable protective clothing, gloves and eye/face protection. S45 - In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.) S25 - Avoid contact with eyes. S16 - Keep away from sources of ignition. |
| UN IDs | UN 2920 8/PG 2 |
| WGK Germany | 3 |
| FLUKA BRAND F CODES | 9-19-21 |
| HS Code | 29189900 |
| Hazard Class | 8 |
| Packing Group | II |
Methoxyacetyl chloride - Reference Information
| NIST chemical information | Information provided by: webbook.nist.gov (external link) |
| EPA chemical information | Information provided by: ofmpub.epa.gov (external link) |
| use | methoxyacetyl chloride is an intermediate of fungicides evil cream and metalaxyl. Used as an intermediate in medicine and dyes |
| production method | its preparation method is to put methanol and flake NaOH into the reaction flask, reflux reaction for 30min, then cool and add a certain amount of chloroacetic acid, heat up the reaction for 2h, evaporate methanol after reflux, then azeotropic dehydration, and cool to below 10 ℃ after water is completely removed, toluene and SOCl2 were added as acylating agents, reacted at about 45 ℃ for 1h, cooled to 20 ℃, and distilled to obtain the product after post-treatment. CH3ONa ClCH2COOH→CH3OCH2COONaCH3OCH2COONa SOCl2→ CH3OCH2COCl NaCl SO2↑ |
Last Update：2024-04-09 20:52:54
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View History
Methoxyacetyl chloride
3-FLUOROBENZENESULFONAMIDE
LDA
A-CHLOROALLYL CHLORIDE
碘化锌 避光
METHOXY METHYL CHLORIDE ( MOM CHLORIDE)
3-FLUOROBENZENESULFONAMIDE
LDA
A-CHLOROALLYL CHLORIDE
碘化锌 避光
METHOXY METHYL CHLORIDE ( MOM CHLORIDE)